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Aging

The progressive and irreversible degradation of elastomer physical properties over time due to environmental exposure. Primary aging mechanisms: thermal oxidation (heat + oxygen break polymer chains and cross-links, causing hardening and cracking), ozone attack (surface cracking perpendicular to stress direction, especially in NR and SBR — concentration as low as 25 ppb causes damage), UV photodegradation (breaks polymer bonds, causes surface chalking and cracking), and chemical attack (solvents, acids, bases causing swelling, softening, or embrittlement). Evaluated by accelerated aging tests: ASTM D573 (air oven aging — measures changes in hardness, tensile, and elongation after 70-168 hours at elevated temperature), ASTM D1149 (ozone resistance), ASTM D750 (rubber deterioration by cut growth). Aging resistance ranking (best to worst): EPDM and silicone (excellent ozone/UV), neoprene (good ozone), NBR (moderate), NR and SBR (poor — require antioxidant/antiozonant protection). Per ISO 188 for heat aging methodology.

What you need to know

  • The progressive and irreversible degradation of elastomer physical properties over time due to environmental exposure.
  • Primary aging mechanisms: thermal oxidation (heat + oxygen break polymer chains and cross-links, causing hardening and cracking), ozone attack (surface cracking perpendicular to stress direction, especially in NR and SBR — concentration as low as 25 ppb causes damage), UV photodegradation (breaks polymer bonds, causes surface chalking and cracking), and chemical attack (solvents, acids, bases causing swelling, softening, or embrittlement).
  • Evaluated by accelerated aging tests: ASTM D573 (air oven aging — measures changes in hardness, tensile, and elongation after 70-168 hours at elevated temperature), ASTM D1149 (ozone resistance), ASTM D750 (rubber deterioration by cut growth).
  • Aging resistance ranking (best to worst): EPDM and silicone (excellent ozone/UV), neoprene (good ozone), NBR (moderate), NR and SBR (poor — require antioxidant/antiozonant protection).
  • Per ISO 188 for heat aging methodology.

Full definition

Aging refers to the progressive and irreversible degradation of elastomer physical properties over time, primarily due to exposure to environmental factors. This phenomenon affects various elastomers differently, with some being more resilient than others. The main aging mechanisms include thermal oxidation, ozone attack, UV photodegradation, and chemical attack. Thermal oxidation occurs when heat and oxygen interact with polymer chains, leading to hardening and cracking. For instance, elastomers subjected to high temperatures in industrial settings may experience accelerated aging, compromising their performance and lifespan. Ozone attack, particularly harmful to natural rubber (NR) and styrene-butadiene rubber (SBR), can cause surface cracking even at low concentrations of ozone (as low as 25 parts per billion). This degradation is often observed in outdoor applications where rubber components are exposed to environmental conditions. UV photodegradation breaks down polymer bonds under sunlight exposure, resulting in surface chalking and cracking, which are detrimental to both aesthetics and functionality.

Chemical attacks from solvents, acids, and bases can lead to swelling, softening, or embrittlement of elastomers. For example, neoprene shows good resistance to certain chemicals but can deteriorate in the presence of strong acids. Evaluating aging resistance is crucial for selecting the right elastomer for specific applications. Accelerated aging tests such as ASTM D573 assess changes in hardness, tensile strength, and elongation after exposure to elevated temperatures for 70-168 hours. ASTM D1149 measures ozone resistance, while ASTM D750 evaluates rubber deterioration through cut growth. The aging resistance of various elastomers ranks from best to worst: EPDM and silicone exhibit excellent ozone and UV resistance, followed by neoprene with good ozone resistance, NBR with moderate resistance, and NR and SBR, which require antioxidant and antiozonant protection to mitigate aging effects. ISO 188 provides a standardized methodology for heat aging assessments, ensuring consistent evaluation across different materials and applications.

What you need to know

  • What you need to know: Aging is an irreversible process that affects elastomers over time due to environmental exposure.
  • Primary aging mechanisms include thermal oxidation, ozone attack, UV photodegradation, and chemical attack.
  • EPDM and silicone rank highest in aging resistance, while NR and SBR perform poorly without protective measures.
  • Accelerated aging tests such as ASTM D573 and ASTM D1149 are critical for evaluating elastomer resilience.
  • Ozone concentrations as low as 25 ppb can cause significant damage to certain elastomers like NR and SBR.

Industrial applications

  • 1In automotive applications, aging affects seals and gaskets, requiring careful material selection for longevity.
  • 2In outdoor structures, rubber components must resist UV and ozone exposure to maintain performance.
  • 3Manufacturers of industrial hoses must consider aging effects when selecting materials for high-temperature applications.
  • 4Electrical insulation products often use EPDM or silicone to ensure long-term durability against environmental degradation.

Common mistakes

  • Neglecting to account for ozone levels when selecting elastomers, leading to premature failure in outdoor applications.
  • Overlooking the impact of temperature on aging, resulting in the selection of materials that degrade too quickly.
  • Failing to perform accelerated aging tests, which can result in unexpected material performance in critical applications.
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Pro tip

Consider using materials with built-in antioxidants and antiozonants to enhance the longevity of elastomers in harsh environments.

Technical standards

  • ASTM D573 - Standard Test Method for Rubber Deterioration—Air Oven Aging.
  • ASTM D1149 - Standard Test Method for Ozone Resistance of Rubber.
  • ASTM D750 - Standard Test Method for Rubber Deterioration by Cut Growth.
  • ISO 188 - Rubber, vulcanized or thermoplastic - Accelerated aging and heat resistance tests.

Suppliers of industrial materials in Mexico

Applicable standards

ASTM D573ASTM D1149ASTM D750ISO 188