Saltar al contenido
PTI LATAMExplorar Portal
Hules

Accelerated Aging

A laboratory test method that exposes rubber specimens to elevated temperatures (typically 70-150°C) in an air oven for defined periods (22, 70, or 168 hours) to simulate long-term degradation and predict service life performance. After aging, specimens are tested for changes in hardness, tensile strength, and elongation at break compared to unaged controls. Per ASTM D573 (air oven aging — most common method) and ISO 188. Acceptance criteria vary by application: typical specifications allow maximum changes of ±15% tensile, -40% elongation, and ±10 points hardness after aging. The Arrhenius equation allows extrapolation of service life from accelerated data: each 10°C increase approximately doubles the degradation rate. For example, 70 hours at 100°C may approximate 1 year at ambient temperature for NR. Additional specialized aging tests: ASTM D1149 (ozone exposure), ASTM D750 (cut growth), ASTM D572 (oxygen bomb). Results are essential for qualifying materials for automotive (SAE, OEM specs), industrial (ISO 14890 for conveyor belt covers), and military applications. Critical for comparing compound formulations during development.

What you need to know

  • A laboratory test method that exposes rubber specimens to elevated temperatures (typically 70-150°C) in an air oven for defined periods (22, 70, or 168 hours) to simulate long-term degradation and predict service life performance.
  • After aging, specimens are tested for changes in hardness, tensile strength, and elongation at break compared to unaged controls.
  • Per ASTM D573 (air oven aging — most common method) and ISO 188.
  • Acceptance criteria vary by application: typical specifications allow maximum changes of ±15% tensile, -40% elongation, and ±10 points hardness after aging.
  • The Arrhenius equation allows extrapolation of service life from accelerated data: each 10°C increase approximately doubles the degradation rate.

Full definition

Accelerated aging is a crucial laboratory test method used to assess the long-term durability and service life of rubber materials, particularly elastomers like SBR, NBR, EPDM, and neoprene. This process involves exposing rubber specimens to elevated temperatures, typically ranging from 70°C to 150°C, in an air oven for specified durations of 22, 70, or 168 hours. The intent is to simulate the effects of prolonged environmental exposure, thereby predicting how these materials will perform over time in real-world applications. The results of accelerated aging tests help engineers and material scientists evaluate the stability and reliability of rubber compounds under stress conditions that mimic actual operating environments.

After the aging process, specimens are subjected to mechanical testing to determine changes in key properties such as hardness, tensile strength, and elongation at break when compared to unaged controls. The acceptance criteria for these changes can vary significantly based on the intended application of the rubber material. Common specifications might allow for maximum changes of ±15% in tensile strength, a reduction of up to 40% in elongation, and a shift of ±10 points in hardness. These parameters are critical for ensuring that rubber products meet performance standards across various industries.

The Arrhenius equation plays a pivotal role in extrapolating the service life of rubber materials from accelerated aging data. It is generally observed that for every 10°C increase in temperature, the degradation rate of the rubber roughly doubles. For instance, aging a rubber sample at 100°C for 70 hours may equate to approximately one year of exposure at ambient temperature for natural rubber (NR). This predictive capability is vital for manufacturers, particularly in sectors like automotive, industrial, and military, where material performance is subject to stringent specifications such as those outlined by SAE and ISO standards.

Additionally, specialized aging tests, such as ASTM D1149 for ozone exposure, ASTM D750 for cut growth, and ASTM D572 for oxygen bomb testing, provide further insights into material performance under specific environmental stresses. The results from these tests are integral for qualifying materials for diverse applications, including automotive components, conveyor belt covers, and military equipment, ensuring that they meet the required durability and safety standards.

What you need to know

  • Accelerated aging tests expose rubber to elevated temperatures (70-150°C) for periods of 22, 70, or 168 hours.
  • Post-aging assessments measure changes in hardness, tensile strength, and elongation, with acceptance criteria varying by application.
  • Typical specifications allow for ±15% tensile strength changes, -40% elongation, and ±10 points hardness after aging.
  • The Arrhenius equation indicates that each 10°C increase roughly doubles the degradation rate of rubber materials.
  • Common norms associated with accelerated aging include ASTM D573 and ISO 188, which guide testing processes.

Formula

t = t₀ × e^(Ea/(R×T))

Industrial applications

  • 1Automotive parts testing for compliance with SAE and OEM specifications.
  • 2Industrial rubber applications requiring durability under extreme conditions, such as conveyor belt covers.
  • 3Military equipment qualification to ensure materials withstand harsh environments.
  • 4Development and comparison of new rubber compound formulations in R&D settings.
  • 5Quality control for rubber products used in critical applications, ensuring they meet performance standards.

Common mistakes

  • Failing to account for the specific aging conditions relevant to the application, leading to misleading results.
  • Not adhering to the established acceptance criteria, which may result in subpar material selection.
  • Overlooking the importance of baseline data from unaged controls, which is essential for accurate comparisons.
  • Neglecting to consider the effects of varying environmental factors on aging, such as humidity and exposure to chemicals.
💡

Pro tip

Always correlate accelerated aging test results with real-world performance data to ensure reliable predictions of material longevity.

Technical standards

  • ASTM D573 - Standard Test Method for Rubber - Accelerated Aging in Air Oven.
  • ISO 188 - Rubber, Accelerated Aging and Heat Resistance Tests.

Suppliers of industrial rubber in Mexico

Applicable standards

ASTM D573ISO 188.ASTM D1149ASTM D750ASTM D572ISO 14890